As with the last example, this formulation uses the pre-emulsified monomer technique.
| 
 Reactor charge  | 
|
| 
 Water  | 
 15.0  | 
| 
 Stabilising colloid  | 
 1.0  | 
| 
 Ammonium persulphate  | 
 0.1  | 
| 
 Pre-emulsion vessel charge:  | 
|
| 
 Water  | 
 44.9  | 
| 
 Styrene  | 
 21.0  | 
| 
 n-Butylacrylate  | 
 12.0  | 
| 
 Hydroxyethyl methacrylate  | 
 5.0  | 
| 
 Emulsifier  | 
 0.5  | 
| 
 Colloid  | 
 0.5  | 
| 
 Total  | 
 100.00  | 
1. Prepare the pre-emulsion by mixing the monomers with the emulsifier and adding colloid dissolved in water.
2. Prepare a solution of stabilising colloid in water in the reaction vessel and add ammonium persulphate.
3. Add 10% of the pre-emulsion to the reaction vessel and heat to 80°C.
4. At 80°C add the remaining pre-emulsion over 2-3 hours.
5. When the addition is complete heat to 90°C and hold at this temperature for 2 hours.
Cool to 50°C and filter via a vibrating screen filter
 21 июля, 2015 
 Malyar 
 Опубликовано в рубрике 