Thermosetting Acrylic Emulsion

As with the last example, this formulation uses the pre-emulsified monomer technique.

FORMULATION 2-5

Reactor charge

Water

15.0

Stabilising colloid

1.0

Ammonium persulphate

0.1

Pre-emulsion vessel charge:

Water

44.9

Styrene

21.0

n-Butylacrylate

12.0

Hydroxyethyl methacrylate

5.0

Emulsifier

0.5

Colloid

0.5

Total

100.00

Procedure

1. Prepare the pre-emulsion by mixing the monomers with the emulsifier and adding colloid dissolved in water.

2. Prepare a solution of stabilising colloid in water in the reaction vessel and add ammonium persulphate.

3. Add 10% of the pre-emulsion to the reaction vessel and heat to 80°C.

4. At 80°C add the remaining pre-emulsion over 2-3 hours.

5. When the addition is complete heat to 90°C and hold at this temperature for 2 hours.

Подпись: 6.Cool to 50°C and filter via a vibrating screen filter

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